Equipment

Bruker Avance DSX 400 WB Spectrometer equipped with: 400 MHz Magnet (9,4T, ultra shield) wide bore. 1H/19F-channel 1000W. X-Kanal (6 - 243MHz;1000W). Y-Kanal (6 - 162MHz;300W). Temperature control unit Solid-state NMR probes 2,5mm CP/MAS-probes(1H/19F; 13C-31P), MAS-frequency ≤ 35kHz, -120°C <T< 150°C. 4mm CP/MAS-triple resonance-probe (1H/19F; 15N, 11B, 13C, 29Si, 31P), MAS-frequency ≤ 15kHz, -120°C <T< 150°C. 7mm CP/MAS-probe (1H/19F; 15N-31P), MAS-frequency ≤ 7kHz, -120°C <T< 150°C. 7mm CP/MAS-probe (1H/19F; 109Ag-29Si), MAS-frequency ≤ 7kHz, -120°C <T< 150°C. 7mm CP/MAS-probe (15N-31P), MAS-frequency ≤ 3kHz, T> 800°C. (120W CO2-Laser heating).

Bruker Avance DPX 300 SB Spectrometer equipped with: 300MHz  Magnet (7,05T, ultra shield) narrow bore. 1H/19F-channel (100W). X-channel (6 - 162MHz; 300W). Temperature control unit. Probes: Liquids: 5mm Broadband-probe (1H; 109Ag-31P), -80°C <T<100°C. Solids: 4mm CP/MAS-Probenkopf (1H/; 15N - 31P), -120°C <T<150°C.