Methodology & Technique Development

Methodology & Technique Development

While the beginnings of Scanning and Transmission Electron Microscopy can now be traced back nearly 100 years to its first realization by Ernst Ruska and Max Knoll in 1931, development and advancement of these techniques never stopped, shifting boarders in accuracy and opening up new possibilities to this day. For example, the enhancements in in-situ instrumentation now not only allows for the investigation of samples under temperatures ranging from close to absolute zero to 1000 °C, checking their electrical bias and observing them within gaseous and liquid environments, but also to dynamically change these environments during the investigation. On the other hand, the introduction of robust direct electron detection cameras boosts the amount of signal that can be collected, which opens up the possibility for rapid acquisition of large amounts of data, reducing beam damage and minimizing the influence of sample drift while offering more information about the sample at the same time.

Not only keeping up with these improvements, but also driving their development forward is a main goal of the StEM. The resulting access to new and improved ways to utilize electron microscopy for the investigation of samples is then applied at StEM for the cooperation with other scientific groups. This not only boost our expertise in these techniques due to the valuable feedback we gain, but first and foremost strengthen their understanding in the materials they are researching.

Schematic illustration of the experiment showing Au-T-G electron emitters under parallel electron-beam irradiation. Emitted electrons are collected by a positively biased electrode.
by Kenan Elibol

The study reveals that electron-beam excitation of metallic nanostructures can produce highly localized electric field intensities sufficient to lower the potential barrier at metal surfaces, thereby enabling electron emission via quantum tunneling. Such findings establish new perspectives for the development of spatially confined electron sources with ultrafast temporal response and contribute to a deeper mechanistic understanding of electron–matter interactions under non-equilibrium conditions.
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